By A. Furstner

ISBN-10: 3527279385

ISBN-13: 9783527279388

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ISBN-13: 9783527281657

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ISBN-10: 3527292845

ISBN-13: 9783527292844

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In conjunction, it is also an important route to many substituted 1,3-dienes. Table 1-18 shows coupling reactions of organozinc and aryl and vinyl halides. It should be noted that organozinc reagents can also be transmetallated to nickel, allowing for the full range of chemistry available to that metal as well. 7 Intramolecular Cyclizations and Conjugate Additions Mediated by Rieke Zinc Rieke zinc is superior to other forms of activated zinc when applied to intramolecular cyclizations and conjugate additions.

Synthesis of spiro-7-lactones. 5]decan-2-one(6) was obtained. Table 1-7 shows representative spiro-ylactones that have been prepared in this way. We have recently reported an extension of this methodology in the production of spiro-d-lactones [37]. Much work has been done to elucidate novel synthetic routes for these types of molecules [38]. In particular, d-substituted d-lactones have recently attracted considerable attention, mainly because molecules of this class include many natural products that exhibit significant biological activity [39].

Whilc the heterogeneous copper metal formed by this process was found to be more reactive than ordinary copper metal, the active copper could not undergo oxidative addition at temperatures low enough to form stable organocopper reagcnts. Consequently, the active copper formed by this method was prone to sinter, giving larger particles upon extended stining or prolonged periods of standing. As a result, the reactivity of the copper metal was reduced. It was also found that substitution of the potassium metal by lithium resulted in much longer reduction times, giving a copper metal that was relatively unreactive.

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Active Metals [chemistry] by A. Furstner


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